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THEORETICAL AND EXPERIMENTAL CHEMISTRY
UDC: 543.24:678.56.06
2015. - T. 29. - No. 1(160). - pp. 31-33
Valeria Viktorovna Gundareva, Yulia Valerievna Ermolenko, Irina Nikolaevna Semenova,
A film polymer sensitive layer (FS) has been developed based on the ion immobilization of alizarin red C (AlR) into a copolymer of methyl methacrylate, ethyl acrylate and a quaternary salt of dimethylaminoethyl methacrylate. The protolytic properties of AlR in a polymer medium were studied. An increase in the acidity of immobilized AlR, expressed in an increase in its first acid dissociation constant, was established.
First page of the article
Links
- Industrial Review. - No. 4 (9). - 2008. - pp. 36 - 38. RF Patent No. 2014107994/15, 03/04/2014.
- Ermolenko Yu.V., Kildeeva N.R., Gridina N.N., Novikova N.G., Mikhailova A.V. Optical sensitive element for determining metal ions in liquid media // Russian Patent No. 149409. 2014. Bull. No. 36.
- Bulatov M.I. Practical guide to photometric methods of analysis / Bulatov M.I., Kalinkin I.P. - 5th ed., revised. - L.: Chemistry, 1986. - P. 244-246.
- Reshetnyak E. A. Protolytic and complex-forming properties of indicators in a gelatin gel medium / Reshetnyak E. A., Nikitina N. A., Loginova L. P., Mchedlov - Petrosyan N. O., Svetlova N. V. // Bulletin of Kharkov national university. - 2005. - No. 669. - P. 67 - 82.
- Savvin S. B. Surface-active substances / Savvin S. B., Chernova R. K., Shtykov S. N. - M.: Nauka, 1991. - P. 84.
Education:
Saratov State University named after N.G. Chernyshevsky, 1971, Chemistry
Dissertations and academic degrees:
Doctor of Chemical Sciences,
Academic title:
Professor at the Department of Analytical Chemistry and Chemical Ecology
Scientific interests:
Analytical chemistry
Total experience:
Experience in specialty:
Work at the university:
Professor, Department of Analytical Chemistry and Chemical Ecology of SSU, from 1991 to the present.
Work history:
In 1981, I was elected to the position of senior lecturer in the same department, in 1984 to the position of associate professor of the department, and in 1988 I was awarded the academic title of associate professor. In November 1990, at the Geochemical Institute of the USSR Academy of Sciences, he defended his doctoral dissertation on the topic: “Solvation effects in systems of organic reagents - their complexes with metals - surfactants” in the specialties 02.00.02 analytical chemistry and 02.00.01 inorganic chemistry.
In April 1991, the USSR Higher Attestation Commission awarded me the academic degree of Doctor of Chemical Sciences.
In December 1991, he was elected to the position of professor in the same department, and in 1993 he received a professor’s certificate in the same department. In 1995 he was elected a corresponding member, and in 1999 a full member of the Russian Academy of Natural Sciences in the “Chemistry” section. From 1995 to 1999, he worked part-time as deputy director for science of the Scientific Research Institute of Chemistry of SSU, in 2000 he was elected to the position of dean of the Faculty of Chemistry of SSU, where he worked until September 2004. Currently, he is a professor at the Department of Analytical Chemistry and Chemical Ecology at the Institute of Chemistry SSU.
Prizes and awards:
State scientific scholarships of the Presidium of the Russian Academy of Sciences: - 1994-1996; 1997-1999 (Decree of the President of the Russian Federation dated September 16, 1993 No. 1372 and Decree of the Government of the Russian Federation dated March 9, 1994)
Certificate of honor from the Ministry for the Development of Sports, Physical Culture and Tourism of the Saratov Region “For active participation in the sports movement of the teaching staff of universities in the region”, order No. 103 dated March 17, 2011.
Certificate of honor from the Ministry of Industry and Energy of the Saratov Region (12/08/11 in connection with the year of chemistry for scientific activities and personnel training)
Diploma of the International Foundation “Scientific Partnership” for high scientific results and training of highly qualified personnel, 2004
Prize of the Russian Foundation for Basic Research (RFBR) for the best popular science article (Nature magazine 2009)
Prize from the publishing house of the Academy of Sciences MAIK-Nauka for the best scientific publication in the Journal of Analytical Chemistry, 2004
Prize of the National Academy of Agricultural Sciences of the Russian Academy of Sciences in Analytical Chemistry 2016 for “For pioneering work in the field of nanoanalytics, significant contributions to luminescent analysis, thin-layer chromatography and other analytical methods”, 2016
Biographical text:
I, Shtykov Sergey Nikolaevich, was born on October 28, 1948 in Krasnoufimsk, Sverdlovsk region. In 1951, my parents moved to the village of Gornyak, three kilometers from the city, and in 1964 our family returned to Krasnoufimsk.
Father, Nikolai Ilyich Shtykov, worked for more than 20 years as an engineer in the chemical analysis laboratory of the Krasnoufimsky Mechanical Plant, and then until his retirement as a teacher at an agricultural technical school. Mother, Margarita Pavlovna Shtykova, first worked as a laboratory assistant in the chemical analysis laboratory of the locomotive depot at the city railway station, and then until retirement in the chemical analysis laboratory of a mechanical plant.
I studied the first two grades of primary school at primary school No. 6 in Krasnoufimsk, grades 3 and 4 in the village of Gornyak, and from grades 5 to 11 at secondary school No. 1 in Krasnoufimsk. After graduating from school, he entered the Faculty of Chemistry of Saratov State University named after N.G. Chernyshevsky (SSU). He combined his studies with skiing, from the 3rd year onwards, for 10 years he was the best skier-racer at SSU; in 1974 he became the champion of Saratov at a distance of 50 km.
After graduating from SSU in 1971, until May 1972, he worked as an engineer at the Research Institute of Chemistry at SSU, then for more than 2 years as a laboratory assistant at the Department of Analytical Chemistry. In September 1974, he was elected as an assistant in the same department and entered correspondence graduate school with the head of the department, associate professor R.K. Chernova. In December 1980, at Perm State University he defended his thesis on the topic: “Study of the influence of surfactants on the chemical and analytical properties of chromophore organic reagents in aqueous solutions” in specialty 02.00.02 - analytical chemistry.
In November 1990, he defended his doctoral dissertation at the Geochemical Institute of the USSR Academy of Sciences
on the topic: “Solvation effects in systems of organic reagents - their complexes with metals - surfactants” in the specialties 02.00.02 analytical chemistry and 02.00.01 inorganic chemistry. In April 1991, the USSR Higher Attestation Commission awarded me the academic degree of Doctor of Chemical Sciences. In 1991, at the Nauka publishing house, together with prof. Savin and prof. R.K. Chernova published the world’s first monograph “Surfactants (Analytical Reagents”), 251 p.
In 1981, I was elected to the position of senior lecturer in the same department, in 1984 to the position of associate professor of the department, and in 1988 I was awarded the academic title of associate professor. In December 1991, he was elected to the position of professor in the same department, and in 1993 he received a professor’s certificate in the same department. In 1995 he was elected a corresponding member, and in 1999 a full member of the Russian Academy of Natural Sciences in the “Chemistry” section. From 1995 to 1999, he worked part-time as Deputy Director for Science of the Research Institute of Chemistry of SSU; in 2000, he was elected to the position of Dean of the Faculty of Chemistry of SSU, where he worked until September 2004.
I accept active participation in public work at the regional, federal and international levels . In 1995, he was elected chairman of the Saratov regional branch of the Russian Chemical Society named after. D.I. Mendeleev, in 1998 a member of the Central Board of the Russian Chemical Society, and in 2007 a member of the Presidium of the Russian Cultural Society (Moscow), from 2011 to 2016. was the chairman of the audit committee of the Presidium. In 2005, the Presidium nominated me as a representative of the Russian Chemical Society in the Division of Analytical Chemistry of the European Association of Chemical and Molecular Sciences (DAC EuCheMS). In 2015, he was elected Chairman of the Nanoanalytics Working Group of DAC EuCheMS. Since 1998, I have been a member of the Scientific Council on Analytical Chemistry (NSAC) of the Russian Academy of Sciences, since 2005, for the third term, a member of the Bureau of the Scientific Council on Analytical Chemistry of the Russian Academy of Sciences, and since 1998, also the chairman of the Volga regional branch of the NSAC. In the Bureau of the National Academy of Agricultural Sciences of the Russian Academy of Sciences, I am deputy chairman of the commission on optical spectral analysis, co-chairman of the commission on nanoanalytics, member of the commission on international relations, on chemical sensors and on the analysis of medical objects. Since 1997, I have been the Chairman of the section “Chemical Luminescence Analysis” of the Scientific Council (SC) on Luminescence of the Department of General Physics and Astronomy. In 2001, he became a member of the “Surfactants” section of the Scientific Council on colloid chemistry and physical and chemical mechanics, and since 2007 he became a member of this Scientific Council. I actively participate in international activities: in 1997 an observer, in 1998-1999 an associate member, and in 2000-2001. – Titular member of the Division of Analytical Chemistry IUPAC (Commission on Spectrochemical and Other Optical Methods of Analysis). Member of the editorial boards of two foreign scientific journals in India and Ukraine. Organized in 2007 the international symposium “ARGUS-2007-Nanoanalytics”, in 1999 the all-Russian conference with international participation “Organic analytical reagents in analysis”, two all-Russian seminars on luminescence (1999 and 2001), two visiting meetings (Bureau NSAA RAS, Volgograd, 2005) and the section of surfactants (Saratov, 1999), two all-Russian conferences of young scientists. Organized the first collective use center in Saratov and SSU. Member of the Academic Council of the Faculty of Chemistry (1995-2004, 2009-present), scientific secretary (2005-2006) of the dissertation council D 212.243.07 and its member since 1993.
Scientific activity. I am the author of the concept of “Nanoanalytics” as a part of analytical chemistry, developing the principles and methods of using nanoobjects and nanotechnologies in the analysis, one of the leading scientists in the field of analytical, physical, colloidal and supramolecular chemistry of organized media. Nanoobjects and nanotechnologies are used for the development of photometric, fluorescent, phosphorimetric methods of analysis, optical and piezoquartz chemical sensors, micellar and magnetic solid-phase extraction, thin-layer, high-performance liquid and gas chromatography. I pay much attention to the study of the thermodynamics of organized media, the kinetics of reactions in them, and the use of the molecular probe method to study them. In total, I am developing more than 10 different scientific areas, reflected in the “Certificate of Scientific Activities”.
The research results were published in 385 works, including 2 monographs, 10 chapters in 8 monographs, 14 textbooks, 340 articles in the central press (including more than 200 in journals of the Higher Attestation Commission), certificates of authorship (Ac) - 6, patents - 9, for 15 developments, certificates of implementation or use of AC were received. In this area, the team under my leadership has prepared and defended 8 doctoral dissertations (3 in physical and 5 in analytical chemistry) and 20 candidate dissertations (including 4 in physical chemistry) over the past 20 years. Currently the supervisor of one candidate's dissertation. Over the past 20 years, in Russia and abroad, he has personally given more than 60 plenary, keynote, invited and oral sectional presentations and, together with colleagues, more than 290 poster presentations at conferences on analytical and colloidal chemistry, physical chemistry of solutions, supramolecular chemistry, luminescence and chromatography.
I am a leader 7 research grants from the Russian Foundation for Basic Research (1994-2016), 4 grants from the Ministry of Education (1996-2001), scientific program “Development of the scientific potential of higher education” in the direction of “New materials and chemical technologies, including nanomaterials and nanotechnologies » Ministry of Education and Science (2005), State Contract No. 02.513.11.3028 Agency for Science and Innovation on the same topic, project part of the Ministry of Education and Science (2014-2016). Two-time winner (1994-96 and 1997-99) of scholarships from the Presidium of the Russian Academy of Sciences, the MAIK Science award for the best publication in 2004 in the Journal of Analytical Chemistry and the RFBR award in 2009 for the best popular science article (Nature magazine) , Soros Professor (2001). He was included in the organizing committees of 6 international (including Euroanalysis-16 (Belgrade) and Euroanalysis-17 (Warsaw)), as well as 10 all-Russian conferences.
Works are widely cited (RSCI-1760 , Hirsch - 18, WoS-1313, Hirsch-16 (www.expertcorps.ru/science/whoiswho/ci86)), students work at universities in Germany, Denmark, Belgium, Italy and Sweden, each having 3-5 trained candidates of science. In 2014, among 7 Russian scientists received the high title " Honored Scientist of the Russian Federation » signed by the President of Russia.
In 1999-2000, he trained for 4 months at the University of Okayama (Japan), in 2009 in Udense (Denmark), in 2012 at Chalmers University of Technology (Sweden), and repeatedly gave invited lectures abroad: in universities in Tokyo, Okayama, Hiroshima (Japan), Chalmers University of Technology (Gothenburg, Sweden), Udense University (Denmark).
In area pedagogical activity I teach courses “History and methodology of chemistry”, “History of chemistry”, “Analytical chemistry of nanoobjects” ”, “Current problems of analytical chemistry”, “Spectroscopic methods of analysis and research”, “Nanochemistry and nanotechnology”, “Nanochemistry”, “Nanotechnology in analytics”, “Methods of chemical identification of substances”, “Certification, metrology and standardization in chemical analysis”, “I am supervisor of more than 70 theses. For the first time, he introduced new spectroscopic methods for the analysis and study of substances at the faculty, as well as methods of capillary gas, high-performance liquid, thin-layer chromatography and the modern method of gas chromatography-mass spectrometry, and applied nanotechnology in the creation of chemical sensors.
Disciplines taught:
History and methodology of chemistry
Methods for chemical identification of substances
Analytical chemistry of nanoobjects (graduate students)
Modern spectroscopic methods for the analysis of new materials (masters)
Application of atomic spectroscopy methods (Bachelors of Law)
Nanochemistry and nanotechnology (1-year master's degree)
History of Chemistry (Bachelors and Chemist Teachers)
Nanochemistry (bachelors in chemistry)
Main scientific publications:
Monographs
- Savvin S.B., Chernova R.K., Shtykov S.N. Surfactants (Analytical reagents). - M.: Nauka, 1991. - 251 p. ISBN 5-02-001346-3
- Shtykov S.N., Popova T.A. Research Institute of Chemistry // In the book: Faculty of Chemistry of Saratov State University. Pages of history. Saratov: Scientific book. 2004. P.38-65. ISBN 5-93888-589-2 / Ed. Shtykova S.N. and Fedotova O.V.
- Shtykov S.N. Faculty of Chemistry In the book: Faculty of Chemistry of Saratov State University. Pages of history. 350 c. Saratov: Scientific book. 2004. P.7-37. ISBN 5-93888-589-2 / Ed. Shtykova S.N. and Fedotova O.V.
- Shtykov S.N. Organized nanosystems in analytical chemistry In the book: Advances in analytical chemistry: to the 75th anniversary of academician Yu.A. Zolotov / resp. re. OK. Shpigun. M.: Nauka, 2007. P.301-308. ISBN 978-5-02-036112-6
- Fundamentals of nanoindustry / Glukhova O.E., Gorokhovsky A.V., Zhukov N.D., Klimov B.N., Shtykov S.N., Shchegolev S.Yu. – Saratov: Publishing house Sarat. Univ., 2009. – 384 p. ISBN 978-5-292-03982-2
- Shtykov S.N. “Supramolecular chemistry and chemical analysis” In the book: “Analytical chemists about themselves and their science.” Chapter 9. pp. 216-236. / Ed.-comp. Yu.A. Zolotov, M.: V.A. Shaposhnik. - Book house “Librokom”. 2011. 320 p. ISBN 978-5-397-01571-4
- Shtykov S.N., Rusanova T.Yu. “Nanosensors” In the book: “Problems of analytical chemistry” / Scientific Council on Analytical Chemistry OKHM RAS. - M.: Nauka, 2010. - T.14: “Chemical sensors”. Ch. 8. P.352-362. / ed. Yu.G.Vlasova M.: Nauka, 2011. 399 p. ISBN 978-5-02-037511-6
- Berezkin V.G., Shtykov S.N., Sumina E.G. Thin Layer Chromatography with a Controlled Gas Phase Influencing on the Separation. In: Advances in Chromatography. Vol.51. Chapter 7. P.281-306. /Ed. by Eli Grushka and Nelu Grinberg. - CRC Press. Taylor & Francis Group, LLC USA. Boca 2013. 316 p. http://www.crcpress.com http://www.taylorandfrancis.com
- Shtykov S.N. Concept, achievements and prospects of nanoanalytics. In the book: Institute of Chemistry. New scientific achievements 2009-2014. Collective monograph. – Saratov: Kubik Publishing House, 2014. – P. 105-110. ISBN 978-5-91818-411-0
- Shtykov S.N. Luminescent analysis in organized media. In the book: “Problems of Analytical Chemistry” / Scientific Council on Analytical Chemistry OKHM RAS. - M.: Nauka, 2015. - T.19: “Luminescent Analysis” / Ed. Romanovskaya G.I. P.121-155. ISBN 978-5-02-039147-5
- Shtykov S.N. Nanoobjects and nanotechnologies in analytical chemistry: definitions, classification, history, main results In the book: “Problems of analytical chemistry” / Scientific Council on Analytical Chemistry OKHM RAS. - M.: Nauka, 2015. - T.20: “Nanoobjects and nanotechnologies in chemical analysis” Chapter 1.1. pp. 11-41. / ed. S.N. Shtykova. 431 p. ISBN 978-5-02-039185-7
- Smirnova T.D., Shtykov S.N. Energy transfer in nanosystems: application in luminescent analysis. In the book: “Problems of analytical chemistry” / Scientific Council on Analytical Chemistry OKHM RAS. - M.: Nauka, 2015. - T.20: “Nanoobjects and nanotechnologies in chemical analysis” Chapter 2.4. pp. 123-150. / ed. S.N. Shtykova. 431 p. ISBN 978-5-02-039185-7
13. Nanoanalytics: Nanoobjects and Nanotechnologies in Analytical Chemistry / Ed. by Sergei Shtykov. De Gruyter. Berlin, Germany, 2018. 446 p. https://www.degruyter.com/view/product/487908
14. Shtykov S.N. Nanoanalytics: definitions, classification, history and primary advances. In: Nanoanalytics: Nanoobjects and Nanotechnologies in Analytical Chemistry. Pt. I: Nanoanalytics: Concepts, Elements, and Peculiarities. Chapter 1. P.3-52 / Ed. by Sergei Shtykov – De Gruyter. Berlin, Germany, 2018. DOI (Chapter): https://doi.org/10.1515/9783110542011-001
ISBN 978-3-11-054006-2; e-ISBN (PDF) 978-3-11-054201-1 www.degruyter.com
15. Smirnova T.D., Shtykov S.N., Zhelobitskaya E.A. Energy transfer in liquid and solid nanoobjects: Application in luminescent analysis. In: Nanoanalytics: Nanoobjects and Nanotechnologies in Analytical Chemistry. Pt. II: Application in spectrometric methods. Chapter 5. P.131-162 / Ed. by Sergei Shtykov – De Gruyter. Berlin, Germany, 2018.
Tutorials
- Kulapina E.G., Shtykov S.N. Tests on analytical chemistry (for 1st year students of the Faculty of Biology). – Saratov, 1978. 21 p.
- Shtykov S.N., Smirnova T.D. Methods of water analysis (Teaching manual for students of the Geological Faculty). – Saratov: Publishing house Sarat. University, 1992.- 116 p. ISBN 5-292-01658-6
- Sumina E.G., Shtykov S.N., Tyurina N.V. Thin layer chromatography. Theoretical foundations and practical application: educational method. allowance. – Saratov: Publishing house Sarat. University, 2002.- 108 p. ( Grif. UMO) ISBN 5-292-02939-4
- Molecular electronics and Langmuir-Blodgett films: textbook. aid for students chem. and physical fak. / B.N. Klimov, S.N. Shtykov, G.Yu. Naumenko, etc.: Under the general editorship. B.N. Klimova, S.N. Shtykova. – Saratov: Publishing house Sarat. University, 2004. – Part 1-116 p. ISBN 5-292-03329-4
- Smirnova T.D., Shtykov S.N. Analytical chemistry: Educational method. aid for students geol. fak. - – Saratov: Publishing house Sarat. Univ., 2004. – 124 p. ISBN 5-292-03267-0
- Sumina E.G., Shtykov S.N., Tyurina N.V. Thin layer chromatography. Theoretical foundations and practical application: textbook. aid for students chem. Faculty.. – Saratov: 2nd ed., add. Publishing house Sarat. University, 2006.- 112 p. ( Vulture UMO) ISBN 5-292-03573-4
- Sumina E.G., Shtykov S.N., Tyurina N.V. Fundamentals of the modifying action of surfactants in liquid chromatography: textbook. aid for students chem. fak. – Saratov: Publishing house Sarat. Univ., 2006.-136 p. ISBN 5-292-03579-3
- Shtykov S.N., Rusanova T.Yu. Problems and trends in the development of modern analytical chemistry: Textbook. aid for students chem. Faculty and students of IDPO, directions. "Chemistry". – Saratov: Publishing house Sarat. University, 2006.- 32 p. ISBN 5-292-03558-0
- Klimov B.N., Shtykov S.N., Gorin D.A., Glukhovskoy E.G., Portnov S.A., Neveshkin A.A., Yashchenok A.M., Inozemtseva O.A., Karagaychev A. L.L., Rumyantseva S.S. Physico-chemistry of nanostructured materials: Guide to laboratory practical work: Textbook for students. fak. nano- and biomedical technologies / Under the general editorship. Klimova B.N., Shtykova S.N. – Saratov: 2008. – 97 p. ISBN 978-5-98116-055-4
- Berezkin V.G., Sumina E.G., Shtykov S.N., Atayan V.Z., Zagniboroda D.A., Nekhoroshev G.A., Chausov A.V. Thin layer chromatography with controlled gas phase influencing the separation. – M.: INHS RAS, 2008. – 39 p.
- Klimov B.N., Shtykov S.N., Gorin D.A., Inozemtseva O.A., Glukhovskoy E.G., Yashchenok A.M., Kolesnikova T.A. Physico-chemistry of nanostructured materials: Textbook. aid for students fak. nano- and biomed. technologies / ed. Klimova B.N., Shtykova S.N. – Saratov: Publishing House “New Wind”, 2009. – 217 p. ISBN 978-5-98116-089-9
- Rusanova T.Yu., Shtykov S.N. Nanotechnologies in optical and piezoquartz sensors: Textbook. aid for students chem. fak. and fact. nano- and biomed. technologies of SSU, - Saratov: “Scientific book”, 2009. – 65 p. ISBN 978-5-9758-1092-2
- Sumina E.G., Shtykov S.N., Zagniboroda D.A., Uglanova V.Z. A new version of controlled gas phase thin layer chromatography. Saratov: Publishing house Saratovsk. un-ta. 2011. 86 p. (electronic edition).
- Sumina E.G., Shtykov S.N., Uglanova V.Z., Kulakova N.V. Thin layer chromatography. Theoretical foundations and practical application // Textbook. 3rd edition, expanded. Saratov: SSU, 2012 . – 128 p. http//library.site.
Articles in the central press and abroad
208.Smirnova T.D., Shtykov S.N., Zhelobitskaya E.A. Energy transfer in liquid and solid nanoobjects: application in luminescent analysis // Physical Sciences Reviews. 2018. V. 3. No. 12. P. DOI: https://doi.org/10.1515/psr-2018-9981
207. Egunova O.R., Shtykov S.N. Concentration of some fluoroquinolone antibiotics using magnetic solid-phase extraction on magnetite nanoparticles // Sorption and Chromatogr. processes. 2018. T. 18. No. 6. P. 825-835.
206. Reshetnikova I.S., Romanevich A.S., Shtykov S.N. Spectrophotometric study of the stability of solutions of quercetin and rutin at different acidity of the environment // Izv. Saratovsk. un-ta. New episode. Chemistry series. Biology. Ecology. 2018. T.18. No. 3. P.256-259. 10.18500/1816-9775-2018-18-3-256-259.
205. Kazimirova K.O. Shtykov S.N. Synthesis and functionalization of magnetic magnetite nanoparticles with chitosan // Izv. Saratovsk. un-ta. New episode. Chemistry series. Biology. Ecology. 2018. T.18. No. 2. P.126-133. DOI: 10.18500/1816-9775-2018-18-2-126-133.
204. Al-Alwani A.J., Kosolapova K.I., Chumakov A.S., Lukyanova V.O., Gorbachev I.A., Kazak A.V., Smirnova A.I., Shtykov S.N., Usol'tseva N.V. , GlukhovskoyE.G.Studying of Surfactant Excess Separation from Non-aqueous Quantum Dots Solution on its Monolayer Formation Process // BioNanoSci. 2018. V. 8. No. 4. P. 1081-1086. DOI 10.1007/s12668-018-0537-0Scopus doi.org/10.1007/s12668-018-0537-0
203 . Svenskaya Y.I., Fattah H., Inozemtseva O.A., Ivanova A.G., Shtykov S.N., Gorin D.A., Parakhonskiy B.V. Key Parameters for Size- and Shape-Controlled Synthesis of Vaterite Particles // Cryst. Growth Des. 2018. V. 18. No. 1. P. 331-337.
DOI: 10.1021/acs.cgd.7b01328 Print Edition ISSN: 1528-7483 Web Edition ISSN: 1528-7505 2016 Impact Factor: 4.055 Web of Science, Scopus
202. Chumakov A.S., Al-Alwani A.J., Gorbachev I.A., Ermakov A.V., Kletsov A.A., Glukhovskoy E.G., Kazak A.V., Usoltseva N.V., Shtykov S.N.Temperature and Mixing Ratio Effects in the Formation of CdSe/CdS/ZnS Quantum Dots with 4′- n-octyl-4-p-Cyanobiphenyl Thin Films // BioNanoSci. 2017. V. 7. No. 4. P. 666-671. DOI: 10.1007/s12668-017-0449-4 Scopus
201. Gorbachev I.A., Shtykov S.N., Brezesinski G., Glukhovskoy E.G. Studying of quantum dots Langmuir monolayers stability at the different subphase temperature // BioNanoSci. 2017. V.7. No. 4. P. 686-691. DOI 10.1007/s12668-017-0404-4 ISSN: 2191-1630 (print version) ISSN: 2191-1649 (electronic version) Scopus
200. Shtykov S.N., Sumina E.G., Uglanova V.Z., Sorokina O.N. Thin-layer chromatography of some amino acids on silica gel in aqueous-organic and modified micellar mobile phases // Zh. analyte chemistry. 2017. T. 72. No. 8. P. 742-750.
199. Kazimirova K.O., Khabibullin V.R., Reshetnikova I.S., Egunova O.R., Shtykov S.N. Concentration of food azo dyes E110 and E124 on magnetite nanoparticles modified with CTAB // Izv. Saratovsk. un-ta. New episode. Chemistry series. Biology. Ecology. 2017. T.17. No. 2. pp. 138-142. DOI10.18500/1816-9775-2017-17-2-138-142
198. Smirnova T.D., Shtykov S.N., Zhelobitskaya E.A., Safarova M.I. Determination of flunixin by the method of sensitized terbium fluorescence in the presence of surfactant micelles // Journal. analyte chemistry. 2017. T. 72. No. 5. P. 481-485.
DOI: 10.7868/S0044450217050127
197. Kartsev V.N., Shtykov S.N. Pankin K.E. To assess the state of the intrinsic macroscopic force field of liquids // Zhurn. structures. chemistry. 2017. T. 58. No. 4. P.759-764. DOI10.15372/JSC20170409
196.Spivakov B.Ya., Shtykov S.N. Department of Analytical Chemistry of the European Association of Chemical and Molecular Sciences // Zavodsk Lab. Diagnostics of materials. 2016. T.82. No. 12. pp. 66-70. ISSN1028-6861 WoS, ScopusIF0.288 RSCI
195. Kobtsov S.N., Shtykov S.N., Mandych V.G., Ilyasov I.Kh., Isaev I.N., Dubrovsky D.S. Titrimetric determination of the mass fraction of the main substance in standard samples of the composition of toxic chemicals and their destruction products // Theoret. applied ecology. 2016. No. 4. P.74-80. ISSN 1995-4301
194. Shtykov S.N. Luminescent analysis (Problems of analytical chemistry). T.19, ed. Romanovskaya G.I. M.: Nauka, 2015. 285 p. // Journal. analyte chemistry. 2016. T. 71. No. 10. P. 1118-1119 DOI: 10.7868/S0044450216100133
193. Magdalena Matczuk, Joanna Legat, Sergei N. Shtykov, Maciej Jarosz, Andrei R. Timerbaev. Characterization of the protein corona of gold nanoparticles by an advanced treatment of CE-ICP-MS data // Electrophoresis. 2016. V. 37. No. 15-16. P.2257-2259. DOI 10.1002/elps.201600152
192. Egunova O.R., Reshetnikova I.S., Shtykov S.N., Mirgorodskaya A.B., Zakharova L.Ya. Sorption-fluorimetric determination of enrofloxacin using magnetite nanoparticles modified with mono- and dicationic surfactants // Sorption and chromatographic processes. 2016. T. 16. No. 4. P. 430-438.
191. Bashko E.S., Shtykov S.N. The influence of the nature of the solvent on the extraction of cannabinoids from plant spice matrices // Sorption and chromatographic processes. 2016. T. 16. No. 4. P. 505-514.
190. Egunova O.R., Reshetnikova I.S., German S.V., Kazimirova K.O., Khabibullin V.R., Zhelobitskaya E.A., Shtykov S.N. Sorption-fluorimetric determination of enrofloxacin using magnetite nanoparticles modified with polyethylenimine // Izv. Saratovsk. un-ta. New episode. Chemistry series. Biology. Ecology. 2016. T.16. No. 1. pp. 48-52.
DOI 10.18500/1816-9775-2016-16-1-48-52
189. Shtykov S.N., Sumina E.G., Atayan V.Z., Berezkin V.G. Thin layer chromatography of benzoic acids with a controlled gas phase: a comparison of different stationary phases // J. Planar Chrom.- Modern TLC. 2016. Vol. 29. No. 1. P. 66-71. DOI 10.1556/1006.2016.29.1.8
188. Egunova O.R., German S.V., Vrabie Ya.A., Shtykov S.N. Synthesis of monodisperse magnetite: influence of temperature, concentration of sodium hydroxide and citric acid on the size of nanoparticles // Izv. Saratovsk. un-ta. New episode. Chemistry series. Biology. Ecology. 2015. T.15. No. 4. pp. 10-15.
187. Al-Saidi M.Z.T., Shtykov S.N. Influence of temperature, isotopic composition of water and ethanol on the tautomeric equilibrium of sulfonated phenylazonaphthols // Izv. Saratovsk. un-ta. New episode. Chemistry series. Biology. Ecology. 2015. T.15. No. 3. P. 5-9.
186. Al-Saidi M.Z.T., Shtykov S.N. Evaluation of the interphase distribution of phenylazonaphthols in the water-surfactant micelle system according to TLC data // Sorption and chromatographic processes. 2015. T. 15. No. 3. P. 443-449. ISSN 1680-0613 IF (RSCI 2013) 0.267
185. Gorbachev I.A., Shtykov S.N., Glukhovskoy E.G. Preparation and fluorescence of multilayer Langmuir-Blodgett films containing CdSe/CdS/ZnS quantum dots // Izv. Saratovsk. un-ta. New episode. Physics series. 2015. T. No. 1. P. 40-45.
184. Batov D.V., Kartsev V.N., Shtykov S.N. Heat capacity, electrical conductivity and structural changes of microemulsions water - sodium dodecyl sulfate - triethanolamine - 1-pentanol - 1,1,2,2-tetrafluorodibromoethane // Zh. str. chemistry. 2015. T.56. No. 2. pp. 282-287.
183. Al-Saidi M.Z.T., Shtykov S.N. Synthesis and spectroscopic study of some phenylazonaphthols // Izv. Saratovsk. un-ta. New episode. Chemistry series. Biology. Ecology. 2015. T.15. No. 1. pp. 9-14.
182. Sumina E.G., Shtykov S.N., Pankratov A.N., Uglanova V.Z., Tsymbal O.A., Danchuk A.I. Separate determination of oleanolic and glycyrrhizic acids by reverse phase thin layer chromatography in aqueous-organic and modified micellar mobile phases // Sorbts. and chromatogr. processes. 2014. T.14. No. 6. P.948-959.
181. Romanov O.E., Budinov S.V., Shtykov S.N. Thin layer chromatography of vitamins A and E on silica gel // Sorbts. and chromatogr. processes. 2014. T.14. No. 4. pp. 563-571.
180. Egunova O.R., Konstantinova T.A., Shtykov S.N. Magnetic magnetite nanoparticles in separation and concentration // 2014. T. 14. Issue.4. WITH.27-34.
179. Shtykov S. Nanoanalytics – a Reply of Analytical Chemistry to the Era of Nanotechnology // J. Anal. Bioanal. Tech. 2014. V. 5. No. 4. P. 35. ISSN: 2155-9872
178. Shtykov S. Supramolecular and nanobiomimetic approach to optimization of analytical reactions // J. Anal. Bioanal. Tech. 2014. V.5. No. 4. P.46. ISSN: 2155-9872
177. Sumina E.G., Shtykov S.N., Sorokina O.N., Prozapas O.N., Uglanova V.Z. Liquid chromatography of some flavonoids on reverse phase in aqueous-organic and modified micellar mobile phases // Zh. analyte chemistry. 2014. T. 69. No. 12. P.1295-1302.
176. Sumina E.G., Shtykov S.N., Sorokina O.N., Uglanova V.Z. Liquid chromatography of some steroid hormones in aqueous-organic, micellar and cyclodextrin mobile phases // Zhurn. analyte chemistry. 2014. T.69. No. 10. pp. 1105-1113.
175. Sumina E.G., Shtykov S.N., Sorokina O.N., Petrakova A.V., Uglanova V.Z., Barysheva S.V. Thin-layer chromatography of flavonoids on silica gel in modified micellar mobile phases based on sodium dodecyl sulfate // Sorbts. and chromatogr. processes. 2014. T.14. No. 1. P.52-64.
174. Shtykov S.N. Nanoanalytics: problems of concept and metrology // Bulletin of the Nizhny Novgorod University. N.I. Lobachevsky. 2013. No. 5. P.55-60.
173. Batov D.V., Kartsev V.N., Shtykov S.N. The influence of temperature on the enthalpy of formation of microemulsions water-o-xylene-triton X-100 // Zhurn. physical chemistry. A. 2013. T.87. No. 3. P.382-386.
172. Parashchenko I.I., Smirnova T.D., Shtykov S.N., Kochubey V.I., Zhukova N.N.
Solid-phase doxycycline-sensitized fluorescence of europium on silica gel in the presence of a surfactant // Zh. analyte chemistry. 2013. T.68. No. 2. P.125-129.
171. Batov D.V., Kartsev V.N., Shtykov S.N. Preparation, heat capacity and flammable properties of water–surfactant–halogenated hydrocarbon microemulsions suitable for creating combined fire extinguishing agents. adj. chemistry. 2012. T. 85. No. 12. P. 1218-1223.
170. Parashchenko I.I., Udalova A.Yu., Smirnova T.D., Shtykov S.N., Zhukova N.N. Express sorption-fluorescence determination of doxycycline in drugs // Izv. Saratovsk. un-ta. New episode. Chemistry series. Biology. Ecology.2012. T. 12. Issue 2. pp. 16 – 20.
169. Kartsev V.N., Shtykov S.N., Pankin K.E., Batov D.V. Molecular forces and internal pressure of liquids // Journal. structures. chemistry. 2012. T.53. No. 6. P.1114-1119.
168. Kartsev V.N., Shtykov S.N., Pankin K.E., Batov D.V. Towards an understanding of the nature of internal pressure of liquids // Monitoring. Science and technology. 2012. No. 2. P.65-70. ISSN 2076-7358 Impact RSCI 0.455
167. Zakharova L.Ya., Valeeva F.G., Ibragimova A.R., Zakharov A.V., Shtykov S.N., Bogomolova I.V., Konovalov A.I. Factors determining the catalytic activity of the mixed micellar system cetyltrimethylammonium bromide-Bridge-35 in the hydrolysis reaction of phosphonic acid ester // Kinetics and catalysis. 2012. T.53. No. 3. pp. 358-367.
166. Shtykov S.N., Kobtsov S.N., Ilyasov I.Kh., Isaev I.N., Dubrovsky D.S., Yazynin S.V. State standard samples of the composition of toxic chemicals and their detoxification products in the system of environmental control and monitoring of facilities for the destruction of chemical weapons // Theoretic. and adj. ecology. 2011. No. 4. P.57-62.
165. Kobtsov S.N., Kuranov G.N., Shtykov S.N., Davydova V.N., Denisov S.N., Zelenikin D.V. Determination of the mass fraction of the main substance in standard samples of the composition of O-alkylmethylphosphonates by potentiometric titration // Zavodsk. lab. Diagnostics of materials. 2011. T.77. No. 12. P.65-70.
164. Vorozheikin S.B., Bashko E.S., Shtykov S.N. Thin layer chromatography of amino acids in micellar mobile phases on silica gel // Sorption and Chromatogr. processes. 2011. T.11. No. 6. P.840-847.
163. Pankin K. E., Ivanova Yu. V., Kuzmina R. I., Shtykov S. N. Comparison of liquid biofuels with oil fuels according to environmental characteristics // Chemistry and technology. fuels and oils. 2011. T.47. No. 3. P.3-6.
162. Pankin K. E., Ivanova Yu. V., Kuzmina R. I., Shtykov S. N. Comparison of liquid biofuels with oil fuels according to operational characteristics // Chemistry and Tekhnol. fuels and oils. 2011. T.47. No. 2. P.23-25.
161. Pankin K.E., Ivanova Yu.V., Kuzmina R.I., Shtykov S.N. Comparison of physicochemical characteristics of biofuel and petroleum products // Chemistry and technology. fuels and oils. 2011. T.47. No. 1. P.8-10.
160. Smirnova T.D., Shtykov S.N., Kochubey V.I., Khryachkova E.I. Excitation energy transfer in europium chelate with doxycycline in the presence of a second ligand in micellar solutions of nonionic surfactants // Optics and Spectrosc. 2011. T.110. No. 1. P.65-71.
159. Kuzmina R.I., Shtykov S.N. Pankin K.E., Ivanova Yu.V., Panina T.G. Pyrogenetic processing of some wood waste and seed shelling waste // Chemistry of plant raw materials. 2010. No. 3. P.61-65.
158. Smirnova T.D., Shtykov S.N., Nevryueva N.V., Zhemerichkin D.A., Parashchenko I.I. Fluorimetric determination of flumequin using sensitized terbium fluorescence in organized media // Khim. pharm. magazine 2010. T.44. No. 11. P.13-16.
157. Shtykov S.N., Smirnova T.D., Nevryueva N.V., Bogomolova I.V. Complexes with energy transfer in organized media for the determination of flumequin in biological objects. Izv. universities Chemistry and chem. technol. 2010. T. 53. No. 11. P. 24-28.
156. Kuzmina R.I., Shtykov S.N., Pankin K.E., Ivanova Yu.V., Panina T.G. High-temperature processing of food waste // Food industry. 2010. No. 7. P.20-21
155. Smirnova T.D., Shtykov S.N., Nevryueva N.V. Reversed-phase HPLC of flumequin and ciprofloxacin in organized media // Sorbts. and chromatogr. processes. 2010. T.10. No. 1. P.142-149.
154. Sorokina O.N., Sumina E.G., Shtykov S.N., Atayan V.Z., Barysheva S.V. Separation of D‑ and L‑ isomers of amino acids by thin layer chromatography in an aqueous mobile phase based on 2‑hydroxypropyl‑‑cyclodextrin // Sorption and Chromatogr. processes. 2010. T.10. No. 1. P.135-141.
153. Kartsev V.N., Polikhronidi N.G., Batov D.V., Shtykov S.N., Stepanov G.V. Model approach to solving problems of thermodynamics of microemulsion systems. Assessing the adequacy of the two-phase model of microemulsions // Journal. physical chemistry. 2010. T. 84. No. 2. P.220-228.
152. Kuzmina R.I., Shtykov S.N. Ivanova Yu.V., Pankin K.E. Calculation of the heat of combustion of biofuel... // Chemistry and technology. fuels and oils. 2009.T.45. No. 6. P. 40-42.
151. Shtykov S.N. In the Saratov regional branch of the Russian Chemical Society named after. D.I. Mendeleev // Chemistry in Russia. 2009. No. 3. P.24-26.
150. Sumina E.G., Vorontsova M.A., Zagniboroda D.A., Shtykov S.N. Influence of the gas phase and surfactant micelles on the separation of phenol derivatives by thin layer chromatography // Sorption and Chromatogr. processes. 2009. T.9. No. 6. P.883-892.
149. Smirnova T.D., Shtykov S.N., Parashchenko I. Fluorimetric determination of europium based on the transfer of excitation energy in organized media // Non-ferrous metals. 2009. No. 11. P. 55-58.
148. Rusanova T.Yu., Kalach A.V., Rumyantseva S.S., Shtykov S.N., Ryzhkina I.S. Determination of vapors of highly volatile organic solvents using piezosensors modified with Langmuir-Blodgett films of calixresorcinarene // Journal. analyte chemistry. 2009. T.64. No. 12. P.1299-1303.
147. Sumina E.G., Shtykov S.N., Berezkin V.G., Zagniboroda D.A., Atayan V.Z. New method of thin layer chromatography with controlled gas phase // Zhurn. analyte chemistry. 2009. T.64. No. 12. P.1256-1264.
146. Smirnova T.D., Nevryueva N.V., Shtykov S.N., Kochubey V.I., Zhemerichkin D.A. Determination of warfarin by the method of sensitized fluorescence using organized media // Journal. analyte chemistry. 2009. T. 64. No. 11. P. 1142-1147.
145. Rusanova T.Yu., Levina N.A., Shtykov S.N. Sol-gel materials with immobilized triphenylmethane dyes as sensitive elements of optical pH sensors // Izv. Saratovsk. un-ta. New episode. Chemistry series. Biology. Ecology. 2009. Vol. 9. Vol. 1. pp. 7–12.
144. Shtykov S.N. Organized media – the world of liquid nanosystems // Nature. 2009. No. 7. P.12-20.
143. Rusanova T.Yu., Taranov V.A., Shtykov S.N., Goryacheva I.Yu. Piezoquartz immunosensor based on Langmuir-Blodgett films for the determination of pyrene in aqueous media. Zavodsk. lab. 2009. T.75. No. 5. P.23-27.
142. Shtykov S.N., Smirnova T.D., Nevryueva N.V., Zhemerichkin D.A. Fluorimetric determination of doxycycline using europium chelate and 1.10-phenanthroline in micellar solutions of Triton X-100 // Izv. universities Chemistry and chem. technol. 2009. T.52. No. 1. P.39-42.
141. Kartsev V.N., Shtykov S.N., Bogomolova I.V., Ryzhov I.P. Thermodynamic stability of microemulsion based on sodium dodecyl sulfate // J. Mol. Liq. 2009. V.145. No. 3. P.173-176.
140. Larionova D.A., Shtykov S.N., Beloglazova N.V., Koroleva E.N. Fluorimetric determination of histamine with o-phthalaldehyde in the presence of nucleophilic agents, surfactant micelles and cyclodextrins // Journal. analyte chemistry. 2008. T. 63. No. 11. P. 1147-1153.
139. Neveshkin A.A., Gorin D.A., Klimov B.N., Rusanova T.Yu., Shtykov S.N. Preparation of nanosized films of calixresorcinarenes based on a combination of polyion assembly and Langmuir-Blodgett methods // Nano- and microsystem technology. 2008. No. 7. P.24-27.
138. Shtykov S.N., Rusanova T.Yu. Nanomaterials and nanotechnologies in chemical and biochemical sensors: capabilities and applications // Ros. chem. magazine 2008. T.52. No. 2. P.92-100.
137. Sumina E.G., Atayan V.Z., Shtykov S.N. Application of cyclodextrin mobile phases in thin layer chromatography of organic reagents of the xanthene and quinoline series // Sorbts. and chromatogr. processes. 2008. T.8. No. 1. P.83-93.
136. Sumina E.G., Shtykov S.N., Zagniboroda D.A., Atayan V.Z., Berezkin V.G. Micellar and ion-pair TLC of ionized compounds in surfactant solutions in the presence of gas modifiers in a chromatographic chamber // Sorbts. and chromatogr. processes. 2008. T.8. No. 1. P.44-49.
135. Gorin D.A., Portnov S.A., Inozemtseva O.A., Karagaichev A.L., Neveshkin A.A., Khlebtsov B.N., Shtykov S.N. Polyelectrolyte microcapsules containing sulfonated b-cyclodextrin molecules in the structure of a nanosized shell // Colloid. magazine 2008. T.70. No. 2. P. 175-180.
134. Neveshkin A.A., Rusanova T.Yu., Podkosov K.V., Serdobintsev A.A., Shtykov S.N., Klimov B.N., Gorin D.A., Rumyantseva S.S., Ryzhkina I.S. The influence of metal ions on the formation and properties of monolayers and nanosized Langmuir-Blodgett films based on aminomethylated calixresorcinarenes. physical chemistry. 2008. T. 82. No. 2. P.316-321.
133. Zakharova L.Ya., Valeeva F.G., Ibragimova A.R., Zakharov V.M., Kudryavtseva L.A., Elistratova Yu.G., Mustafina A.R., Konovalov A.I., Shtykov S.N., Bogomolova I.V. Properties of the binary micellar system sodium dodecyl sulfate - bridge-35 and their effect on the alkaline hydrolysis of o-ethyl-o-p-ni// Colloid. magazine 2007. T. 69. No. 6. P. 766-774.
132. Shtykov S.N. Organized nanosystems in analytical chemistry // Uspekhi analyt. chemistry: to the 75th anniversary of academician. Yu.A. Zolotova. M.: Nauka, 2007. P.301-308.
131. Gorin D.A., Neveshkin A.A., Rusanova T.Yu., Shtykov S.N., Klimov B.N., Podkosov K.V., Ryzhkina I.S., Lukashenko S.S. Monolayers and Langmuir-Blodgett films based on diphilic aminomethylated calixresorcinarenes // Nano and microsystem technology. 2007. No. 1.P.57-60.
130. Mentov E.V., Korotkov S.G., Shtykov S.N., Kuzmina R.I. Determination of thiophene in natural gas and in the air of the working area by capillary gas chromatography with a flame ionization detector // Sorbts. and chromatogr. processes. 2007. T.7. No. 4. P.603-609.
129. Berezkin V.G., Chausov A.V., Shtykov S.N., Sumina E.G. The influence of changes in the composition of the gas phase surrounding the plate on the retention of separated components in TLC // Sorbts. and chromatogr. processes. 2007. T.7. No. 1. P. 106-110.
128. Berezkin V.G., Sumina E.G., Shtykov S.N., Zagniboroda D.A., Atayan V.Z. Dynamic modification of chromatographic separation in TLC based on the properties of the gas phase // Sorbts. and chromatogr. processes. 2007. T.7. No. 1. P.28-32.
127. Inozemtseva O.A., Pipin S.V., Shtykov S.N., Kurochkina G.I., Grachev M.K., Pankin K.E. Synthesis of amphiphilic bromo derivatives of b-cyclodextrin as potential receptor molecules for phosphorescence at room temperature. Izv. Sarat. un-ta. New episode. Chemistry series. Biology. Ecology. 2007. T.7. Vol. 1.S. 15-20.
126. Yashchenok A.M., Gorin D.A., Pankin K.E., Lomova M.V., Shtykov S.N., Klimov B.N., Kurochkina G.I., Grachev M.K. Transfer coefficient of Langmuir-Blodgett films as an indicator of the surface of monocrystalline silicon modified with polyion layers // Physics and technology of semiconductors 2007. Vol. 41. No. 6. P.706-710.
125. Shtykov S.N. Kalach A.V., Pankin K.E., Rusanova T.Yu., Selemenev V.F. Application of Langmuir-Blodgett films as modifiers of piezoresonant sensors // Journal. analyte chemistry. 2007. T.62. No. 5. P. 544-548.
124. Shtykov S.N., Kalashnikova N.V., Smirnova T.D., Zhemerichkin D.A. Determination of ciprofloxacin and enrofloxacin by the method of sensitized europium fluorescence in the presence of a second ligand and micelles of anionic surfactants // Journal. analyte chemistry. 2007. T.62. No. 2. P.153-157.
123. Kartsev V.N., Tsepulin V.V., Shtykov S.N., Pankin K.E. Piezometric assessment of the effect of 2-hydroxypropyl-b-cyclodextrin molecules on the network of hydrogen bonds of water // Journal. structures. chemistry. 2006. T. 47. Appendix. P.85-88.
122. Shtykov S.N., Kalashnikova N.V., Smirnova T.D., Konyukhova Yu.G. Complexes with energy transfer in an excited state in organized media for the fluorimetric determination of biologically active antibiotics // Biomedical technologies and radioelectronics. 2006. No. 12. P. 4-9.
121. Shtykov S.N., Kalashnikova N.V., Smirnova T.D., Zhemerichkin D.A. Fluorimetric method for the determination of norfloxacin, based on the phenomenon of energy transfer. Izv. universities Chemistry and chem. technol. 2006. T.49. No. 7. P.27-30.
120. Safarova M.I., Sosnovskaya T.I., Shtykov S.N. Complexation of iron III with salicylic acid in solutions of surfactants // Saratov Military Institute of Radiation, Chemical and Biological Protection: Coll. scientific works Vol. 6. Saratov 2006. P.37-39.
119. Inozemtseva O.A., Shtykov S.N., Pankin K.E. Kurochkina G.I. Grachev M.K. Monolayers and Langmuir-Blodgett films of amphiphilic b-cyclodextrin derivatives as potential receptor molecules for optical and piezoquartz sensors // Sorbts. and chromatogr. processes. 2006. T6. No. 6. Part 2. P.1080-1085.
118. Shtykov S.N., Bylinkin Y.G., Smirnova T.D., Kalashnikova N., Zhemerichkin D.A. Fluorescence study on the system Eu – oxytetracycline – co-ligand – sodium dodecylbenzene sulfonate micelles and its analytical application // Proc. SPIE 2006. V.6165. P.61650Q1-61650Q7.
117. Berezkin V.G., Sumina E.G., Shtykov S.N., Atayan V.Z., Zagniboroda D.A., Nekhoroshev G.A. Effect of chamber gas phase on mobile phase pH and on separation efficiency in TLC: A new mode of chromatography // Chromatographia 2006. V. 64. No. 1-2. P.105-108.
116. A.M. Yashchenok, D.A. Gorin, K.E. Pankin, A.A. Neveshkin, M.A. Getsman, B.N. Klimov, S.N. Shtykov Electrophysical properties of MIS structures containing nanosized Langmuir-Blodgett films based on b-cyclodextrin // Zhurn. tech. physics. 2006. T.76. No. 4. pp. 105-107.
115. Shtykov S.N., Kartsev V.N., Sumina E.G., Smirnova T.D., Rusanova T.Yu., Goryacheva I.Yu., Pankin K.E. Application of organized media and principles of supramolecular chemistry in chemical analysis // Vestn. Moscow state regional un-ta. Ser. Natural Sciences. No. 1 M.: publishing house MGOU. 2006. pp. 14-26.
114. Shtykov S.N. In the Scientific Council on Analytical Chemistry of the Russian Academy of Sciences // Journal. analyte chemistry. 2006. T. 61. No. 7. P.767-769.
113. Larionova D.A., Shtykov S.N., Koroleva E.N., Beloglazova N.V. Determination of histamine in fish products by thin layer chromatography and fluorimetry // Sorbts. and chromatogr. processes. 2006. T. 6. No. 2. P.337-342.
112. Shtykov S.N., Rusanova T.Yu., Kalach A.V., Pankin K.E. Application of Langmuir Blodgett Films as Modifiers of Piezoresonance sensors // Sensors and Actuators B 2006. V. 114. P.497-499.
111. Berezkin V.G., Sumina E.G., Shtykov S.N., Zagniboroda D.A., Atayan V.Z. A new method of thin layer chromatography of ionizable compounds, based on changes in the acidity of the mobile phase during the elution process. Dokl. AN. 2006. T. 407. No. 3. P.349-351.
110. Savvin S.B., Shtykov S.N., Mikhailova A.V. Organic reagents in spectrophotometric analysis // Advances in Chemistry. 2006. T.75. No. 4. P.380-389.
109. Safarova M.I., Shtykov S.N., Okunev A.V. Influence of the length of the oxyethylene chain of nonionic surfactants on the azoquinone hydrazone tautomerism of the sulfonate derivative of phenylazonaphthol // Saratovsk. Military Institute of Radiation, Chemistry and biological protection: Sat. scientific works Issue 5. Saratov-2005. P.27-31.
108. Shtykov S.N. Organized media as an alternative to traditional organic solvents in chemical analysis // Izv. Saratovsk. un-ta. 2005. T.5. Ser. Chemistry, biology, ecology. Vol. 1. P.47-52.
107. Sumina E.G., Shtykov S.N., Atayan V.Z. Cyclodextrins as modifiers of mobile and stationary phases in liquid chromatography // Sorbts. and chromatogr. processes. 2005. T.5. No. 5. pp. 719-735.
106. Kartsev V.N., Shtykov S.N., Shtykova L.S. Precision dilatometry of microemulsions with anionic surfactants // Colloid. magazine 2005. T.67. No. 4. P.479-484.
105. Goryacheva I. Yu. Shtykov S.N., Loginov A.S., Panteleeva I.V. Preconcentration and Fluorimetric Determination of Polycyclic Aromatic Hydrocarbons Based on the Acid-induced cloud-point Extraction with Sodium Dodecylsulphate // Anal. Bioanal. Chem. 2005. V. 382. P.1413-1418.
104. Mirgorodskaya A.B., Kudryavtseva L.A., Shtykova L.S., Bogomolova I.V., Shtykov S.N. Aminolysis of carboxylic acid esters in direct, bicontinuous and inverted microemulsions based on cetyltrimethylammonium bromide // Journal. general chemistry 2005. T.75. No. 7. pp.1171-1176.
103. Zakharova L.Ya., Valeeva F.G., Zakharov A.V., Kharlampidi H.E., Kudryavtseva L.A., Shtykov S.N., Bogomolova I.V. Micelle-forming properties, micropolarity and catalytic effect of the binary micellar system sodium dodecyl sulfate - Bridge-35 // Sorbts. and chromatogr. processes. 2005. T. 5. No. 3. P.398-406.
102. Shtykov S.N., Smirnova T.D., Bylinkin Yu.G., Zhemerichkin D.A. Fluorimetric determination of tetracyclines using europium chelate with 1.10-phenanthroline in micellar solutions of anionic surfactants // Journal. analyte chemistry. 2005.T. 60. No. 1. P.30-34.
101. Zakharova L.Ya., Ibragimova A.R., Valeeva F.G., Kudryavtseva L.A., Konovalov A.I., Shtykov S.N., Shtykova L.S., Bogomolova I.V. The reactivity and microscopic polarity studies in the sodium dodecyl sulfate based reversed micellar system // J. Mol. Liq. 2005. V. 116. P.83-91.
100. Sumina E.G., Shtykov S.N., Tyurina N.V. Thin-layer chromatography of chromophore indicators, chelating reagents and metal chelates in surfactant solutions // Sorbts. and chromatogr. processes. 2004. T. 4. No. 6. P.750-763.
99. Shtykov S.N., Beloliptseva G.M., Larionova D.A. Express method of sample preparation of food objects for fluorimetric determination of histamine // Izv. Universities. Chemistry and chem. technol. 2004. T.47. No. 7 pp. 123-127.
98. Goryacheva I.Yu., Shtykov S.N., Fedorenko E.V., Melnikov G.V. Influence of internal and external heavy atom on the phosphorescence of pyrene at room temperature in micellar solutions of sodium dodecyl sulfate // Zh. physical chemistry. 2004. T. 78. No. 12 P.2264-2267.
97. Shtikov S.M. Centers were organized as an alternative to traditional retailers // Chemistry. 2004, No. 7. P.2-5.
96. Shtykov S.N., Klimov B.N., Gorin D.A., Pankin K.E., Getsman M.A., Kurochkina G.I., Glazyrin A.E., Grachev M.K. Monomolecular layers and Langmuir-Blodgett films based on b-cyclodextrins with different numbers of alkyl chains // Zh. physical chemistry. 2004. T. 78. No. 10. P. 1852-1857.
95. Shtykov S.N., Korenman Ya.I., Rusanova T.Yu., Gorin D.A., Kalach A.V., Pankin K.E. Langmuir-Blodgett films as effective modifiers of piezoquartz sensors // Dokl. AN 2004. T. 396. No. 4. P.508-510.
94. Goryacheva I.Yu., Shtykov S.N., Fedorenko E.V., Melnikov G.V. Factors affecting on the determination of polycyclic aromatic hydrocarbons by sensitized room temperature phosphorescence // Proc. 8 th Anal. Russian-German-Ukrainian Symp. (ARGUS)/Ed. by N.H. Bings. 2003. P.67-72.
93. Ibragimova A.R., Valeeva F.G., Zakharova L.Ya., Kudryavtseva L.A., Azancheev N.M., Shtykov S.N., Shtykova L.S., Bogomolova I.V. Catalytic properties of the reverse micellar system sodium dodecyl sulfate – butanol – water. // Journal. physical chemistry. 2004. T.78. No. 7. P.1185-1190.
92. Shtykov S.N., Smirnova T.D., Bylinkin Yu.G. Determination of adenosine triphosphoric acid by the quenching of fluorescence of europium (III) diketonate chelate in Bridge-35 micelles // Zh. analyte chemistry. 2004. T. 59. No. 5. P. 495-499.
91. Shtykov S.N., Klimov B.N., Gorin D.A., Getsman M.A., Pankin K.E. Ellipsometric study of polyamide and polyimide Langmuir-Blodgett films // Journal. physical chemistry. 2004. T. 78. No. 3. P. 503-506.
90. Shtykov S.N., Rusanova T.Yu., Smirnova T.D., Gorin D.A. Sensitive element of an optical sensor based on benzopurpurine 4B for determining the acidity of etching solutions // Journal. analyte chemistry. 2004. T. 59. No. 2. P.198-201.
89. Korenman Ya.I., Kalach A.V., Pankin K.E., Shtykov S.N. Determination of C 1 -C 3 nitroalkanes in air using Langmuir-Blodgett films based on b-cyclodextrin // Sensor 2002. No. 4. P. 32-35.
88. Kartsev V.N., Rodnikova M.N., Shtykov S.N. On internal pressure, its temperature dependence and the structure of liquid-phase systems // Zhurn. str. chemistry. 2004. T.45. No. 1. P. 99-102.
87. Kartsev V.N., Rodnikova M.N., Shtykov S.N. Inversion of the temperature coefficient of internal pressure and structural organization of liquid-phase systems // Journal. str. chemistry. 2004. T.45. No. 1. P. 94-98.
86. Batov D.V., Kartsev V.N., Shtykova L.S., Shtykov S.N. Thermal properties of water-n-octane-pentanol-sodium dodecyl sulfate microemulsions at 298.15 K // Izv. universities Chemistry and chem. technol. 2003. T.46. No. 7. P.7-10.
85. Sumina E.G., Shtykov S.N., Barysheva S.V. Hydrophobic and salt effects in ion-pair chromatography of acidic and basic benzene derivatives in the presence of surfactants and strong electrolytes // Sorbts. and chromatogr. processes. 2003. T.3. No. 5. pp. 586-598.
84. Shtykov S.N. Organized media as an alternative to traditional solvents // UNIVERSITATES. 2003. No. 2. P. 20-25.
83. Shtykov S.N., Goryacheva I.Yu., Shtykova L.S. Micelles and microemulsions in separation and concentration // Journal. analyte chemistry. 2003. T.58. No. 7. pp. 732-733.
82. Atayan V.Z., Sumina E.G., Shtykov S.N. Determination of food dyes by TLC with cyclodextrin mobile phases // Journal. analyte chemistry. 2003. T. 58. No. 7. P. 721-722.
81. Atayan V.Z., Sumina E.G., Shtykov S.N. Thin-layer chromatography of azo compounds in mobile phases modified with cyclodextrins // Sorbts. and chromatogr. processes. 2003. T. 3. No. 4. pp. 392-398.
80. Sumina E.G., Shtykov S.N., Tyurina N.V. Ion-pair thin-layer chromatography of the main triphenylmethane and xanthene reagents in surfactant solutions // Sorbts. and chromatogr. processes. 2003. T. 3. No. 4. pp. 412-417.
79. Batov D.V., Kartsev V.N., Shtykova L.S., Shtykov S.N. Calorimetric study of aqueous solutions of sodium dodecyl sulfate and Triton X-100 at 298.15 K // Izv. universities Chemistry and chem. technol. 2003. T.46. No. 6. P. 80-82.
78. Shtykov S.N., Okunev A.V., Safarova M.I. Tautomeric equilibrium of sulfo derivatives of 4-(phenylazo)-1-naphthols in micellar solutions of nonionic surfactants // Journal. analyte chemistry. 2003. T. 58. No. 11 P. 1154-1161.
77. Sumina E.G., Shtykov S.N., Tyurina N.V. Surfactants in thin layer chromatography: a review // Journal. analyte chemistry. 2003. T.58. No. 8. pp. 809-819.
76. Kartsev V.N., Rodnikova M.N., Shtykov S.N., Bartel I. Internal pressure of binary aqueous solutions of diamines, monoethanolamine and diols // Zh. physical Chemistry 2003. T. 77. No. 8. P. 1456-1462.
75. Shtykov S.N., Sumina E.G., Tyurina N.V. Micellar thin-layer chromatography: features and analytical capabilities // Ros. chem. magazine 2003 T.47. No. 1. P.119-126.
74. Goryacheva I., Shtykov S., Melnikov G., Fedorenko E. Analysis of polycyclic aromatic hydrocarbons by sensitized room temperature phosphorescence // Environ. Chem. Lett. 2003. No. 1. P. 82-85.
73. Shtykov S.N., Rusanova T.Yu. Langmuir-Blodgett films as matrices of sensitive elements of optical sensors of solution acidity // Dokl. RAS. 2003. T.388. No. 5. pp. 643-645.
72. Kartsev V.N., Shtykov S.N., Sineva A.V., Tsepulin V.V. Shtykova L.S. Volumetric and transport properties of microemulsions water/n-octane/sodium dodecyl sulfate/n-pentanol // Colloid. magazine 2003. T. 65. No. 3. P.429-432.
71. Korenman Ya.I., Shtykov S.N., Kalach A.V., Pankin K.E., Rusanova T.Yu., Kurochkina G.I., Glazyrin A.E., Grachev M.K. b-Cyclodextrin as an effective modifier of piezoquartz sensors // Izv. universities Chemistry and chem. technol. 2003. T.46. No. 2. P.31-35.
70. Shtykov S.N., Melnikov G.V., Shtykova L.S. Fluorimetric and conductometric study of microemulsions water-sodium dodecyl sulfate-octane-pentanol // Izv. RAS. Ser. chem.2003. T. 52. No. 2. P. 381-385.
69. Melnikov G.V., Shtykov S.N., Zaev E.E., Shtykova L.S. Features of deactivation of photoexcited states of trypaflavin and PAH molecules in aqueous micellar solutions of sodium dodecyl sulfate with the addition of cosurfactants // Journal. physical Chemistry 2003. T. 77. No. 2. P.345-348.
68. Goryacheva I.Yu., Melnikov G.V., Shtykov S.N. Influence of external heavy atoms on the luminescent properties of pyrene in individual and mixed micelles of Triton X-100 and sodium dodecyl sulfate // Zh. physical chemistry. 2003. T. 77. No. 2. P. 281-284.
67. Sumina E.G., Shtykov S.N., Dorofeeva S.V. Ion-pair liquid chromatography of nitrogen-containing medicinal substances in the presence of surfactants and strong electrolytes // Izv. Universities. Chemistry and chem. technol. 2002. T.45. No. 6. P.133-136.
66. Melnikov G.V., Rusanova T.Yu., Shtykov S.N. Optical sensors based on phosphorescence at room temperature // Sensors and systems. 2002. No. 11. pp. 29-31.
65. Korenman Ya.I., Kalach A.V., Rusanova T.Yu., Shtykov S.N. Application of piezosensors based on Langmuir-Blodgett films of arachidic acid for detecting nitroalkanes in air // Sensor. 2002. No. 2. P.14-17.
64. Melnikov G.V., Shtykov S.N., Shtykova L.S., Goryacheva I.Yu., Abramova E.V. Influence of the composition of aqueous-organic media on the efficiency of the formation of excimers of polycyclic aromatic hydrocarbons in singlet and triplet states // Zhurn. physical Chemistry 2002. T. 76. No. 10. P. 1790-1793.
63. Sumina E.G., Shtykov S.N., Tyurina N.V. Micellar thin layer chromatography. Physico-chemical features of the method // Journal. physical chemistry. 2002. T. 76 No. 9. P. 1683-1688.
62. Kartsev V.N., Rodnikova M.N., Bartel I., Shtykov S.N. On the temperature dependence of the internal pressure of liquids // Journal. physical Chemistry 2002. T. 76. No. 6. P. 1016-1018.
61. Zaev E.E., Melnikov G.V., Shtykov S.N., Shtykova L.S. Adsorption of aliphatic alcohols on sodium dodecyl sulfate micelles from data on fluorescence quenching // Zh. physical chemistry. 2002. T.76. No. 5. P.912-914.
60. Levshin L.V., Melnikov G.V., Shtykov S.N., Goryacheva I.Yu. Factors determining the chemical binding of oxygen in micellar solutions of sodium dodecyl sulfate // Journal. physical chemistry. 2002 T. 76. No. 4. P.699-703.
59. Shtykov S.N., Smirnova T.D., Bylinkin Yu.G. Sensitized fluorescence of the thenoyl trifluoroacetonate complex of europium with some organic bases in micellar solutions of nonionic surfactants. Izv. universities Chemistry and chem. technol. 2002. T. No. 2. P. 96-100.
58. Kartsev V.N., Shtykov S.N., Tsepulin V.V., Shtykova L.S. Batov D.V., Antonova O.A., Korolev V.P. Features of bulk properties of aqueous solutions of micelle-forming surfactants // SOFW-Journal (Russian version). 2002. No. 2. P.52-57.
57. Shtykov S.N. Chemical analysis in nanoreactors: basic concepts and applications // Journal. analyte chemistry. 2002. T. 57. No. 10. P. 1018-1028.
56. Shtykov S.N., Sumina E.G., Tupitsyn N.M., Novak Yu.M., Rusanova T.Yu. Training center for retraining specialists - analysts // Journal. analyte chemistry. 2002. T. 57. No. 8. P. 885-886.
55. Shtykov S.N., Sumina E.G., Tyurina N.V. Calculation of interphase distribution coefficients of organic reagents in micellar TLC // Zhurn. analyte chemistry. 2002. T. 57. No. 4. P. 383-387.
54. Sumina E.G., Shtykov S.N., Dorofeeva S.V. Ion-pair reversed-phase thin-layer and high-performance liquid chromatography of benzoic acids // Journal. analyte chemistry. 2002. T. 57. No. 3. P. 257-261.
53. Melnikov G.V., Shtykov S.N., Kosarev.A.V., Goryacheva I.Yu. Triplet-triplet energy transfer between trypaflavin and pyrene in aqueous micellar solutions of sodium dodecyl sulfate // Izv. Universities. Chemistry and chem. technol. 2001 T.44. No. 6. P.18-22.
52. Melnikov G., Shtykov S., Goryacheva I. Sensitized room temperature phosphorescence of pyrene in sodium dodecylsulphate micelles with triphaflavine as energy donor // Anal. Chim. Acta. 2001. V. 439. No. 1. P. 81-86.
51. Shtykov S.N. Educational and scientific complex in chemical sciences of SSU // Izv. Sarat. un-ta. New episode. 2001. T.1., Issue 1. P.44-52.
50. Shtykov S.N. Organized environments – a strategy based on the principles of biosimilarity in analytical chemistry // Visnik Kharkiv. National Univ. No. 495. Chemistry. VIP. 6 (29). Kharkiv. 2000. pp. 9-14.
49. Sumina E.G., Shtykov S.N., Tyurina N.V. Hydrophobic TLC of phenolcarboxylic acids of the triphenylmethane series in surfactant micelles. Izv. Universities. Chemistry and chem. technol. 2001. T. 44. No. 4. P. 10-13.
48. Melnikov G.V., Rusanova T.Yu., Shtykov S.N. Influence of heavy metal salts on solid-phase phosphorescence at room temperature of pyrene adsorbed on filter paper. Izv. Universities. Chemistry and chem. technol. 2001. T. 44. No. 4. P. 13-16.
47. Melnikov G.V., Shtykov S.N., Goryacheva I.Yu., Fedorenko E.V. Luminescent properties of acridine dyes in micellar solutions of sodium dodecyl sulfate // Izv. RAS. Ser. chem. 2001. No. 6 P. 944-946.
46. Shtykov S.N., Smirnova T.D., Molchanova Yu.V. Synergistic effects in the europium-thenoyltrifluoroacetone-phenanthroline system in micelles of surfactant block copolymers and their analytical significance // Journal. analyte chemistry. 2001. T. 56. No. 10 P. 1052-1056.
45. Burmistrova N.A., Mushtakova S.P., Shtykov S.N., Kozhina L.F., Rodnikova V.N. Physicochemical and analytical properties of systems based on redox reagents of the diphenylamine series, modified with surfactants. Zhurn. analyte chemistry. 2001. T.56. No. 7. pp. 732-738.
44. Klimov B.N., Naumenko G.Yu., Vorontsova N.N., Glukhovskoy E.G., Gorin D.A., Kalashnikov S.N., Shtykov S.N., Rusanova T.Yu. Preparation and study of the physicochemical properties of Langmuir-Blodgett films based on polyamide acid // Izv. universities Ser. mater. electron. technology. 2001. No. 1. P.35-38.
43. Sumina E.G., Ermolaeva E.V., Tyurina N.V., Shtykov S.N. The use of surfactants for the modification of mobile and stationary phases in the determination of food dyes by TLC // Zavodsk. lab. 2001. T. 67. No. 5. P. 5-8.
42. Sumina E.G., Smushkina E.V., Shtykov S.N., Tyurina N.V. Application of micellar mobile phases to assess the purity of xylenol orange preparations // Zavodsk. lab. 2001. T. 67. No. 10. P. 13-15.
41. Kartsev V.N., Shtykov S.N., Tsepulin V.V., Shtykova L.S. Volumetric properties of microemulsions n-heptane – water – sodium dodecyl sulfate – n-pentanol. // Colloid. magazine 2000. T.62. No. 6. pp. 860-862.
40. Shtykov S.N., Sumina E.G., Tyurina N.V. Micellar mobile phases in TLC separation of some transition metal ions and their 1,3-diketonates // J. Planar Chromatogr. – Modern TLC. 2000. V.13. No. 4. P. 264-268.
39. Burmistrova N.A., Mushtakova S.P., Shtykov S.N., Rodnikova V.N., Kozhina L.F. The influence of surfactants on the acid-base and redox properties of reagents of the diphenylamine series. Izv. RAS. Ser. chem. 2000. No. 8. pp.1386-1388.
38. Melnikov G.V., Shtykov S.N., Shtykova L.S., Goryacheva I.Yu. Sensitized phosphorescence of pyrene molecules, enhanced by the heavy atom effect in a water-heptane-sodium dodecyl sulfate-pentanol microemulsion. Izv. RAS. Ser. chem. 2000. No. 9. pp. 1529-1532.
37. Shtykov S.N., Sumina E.G., Smushkina E.V., Tyurina N.V. Dynamic and static modification of the stationary phases with surfactants in TLC: a comparative study // J. Planar Chromatogr. – Modern TLC. 2000. V.13. No. 3. P. 182-186.
36. Goryacheva I.Yu., Melnikov G.V., Shtykov S.N. Acridine dyes in the triplet state as reagents for the selective phosphorimetric determination of polycyclic aromatic hydrocarbons in sodium dodecyl sulfate micelles. analyte chemistry. 2000. T.55. N 9. pp. 971-975.
35. Shtykov S.N., Goryacheva I.Yu., Melnikov G.V., Ponomarev A.S. Phosphorimetric determination of polycyclic aromatic hydrocarbons in gasoline // Journal. analyte chemistry. 2000. T. 55. No. 8. pp.883-887.
34. Shtykov S.N. Surfactants in analysis. Main achievements and development trends // Journal. analyte chemistry. 2000. T. 55. No. 7. P. 679-686.
33. Kartsev V.N., Shtykov S.N., Tsepulin V.V., Malova M.I., Shtykova L.S. Volumetric properties of aqueous solutions of Triton X-100 // Journal. physical chemistry. 2000. T.74. No. 12. pp. 2285-2288.
32. Melnikov G., Shtykov S., Goryacheva I. Room temperature phosphorescence as an indicator of triplet-triplet energy transfer between dyes and polycyclic aromatic hydrocarbons solubilized in anionic micelles // Eds V.L. Derbov, L.A. Melnikov, V.P. Ruabukho. Proc. SPIE. Vol. 4002. Bellingham, 2000. P.217-224.
31. Ponomarev A.S., Shtykov S.N. Determination of pesticides and physiologically active compounds by capillary gas chromatography with an atomic emission detector in the absence of standards for the substances being determined // Zhurn. analyte chemistry. 2000. T. 55. No. 1 P. 54-58.
30. Shtykov S.N., Klimov B.I., Naumenko G.Yu., Melnikov G.V., Smirnova T.D., Rusanova T.Yu., Gorin D.A., Glukhovskoy E.G. Preparation and study of a Langmuir-Blodgett film based on polyamide acid containing a rhodamine dye. physical chemistry. 1999. T. 73. No. 9. C. 1711-1713.
29. Shtykov S.N., Sumina E.G., Smushkina E.V., Tyurina N.V. Thin layer chromatography of fluoresceine derivatives on direct and reversed stationary phases with aqueous micellar solutions // J. Planar Chromatogr. – Modern TLC. 1999. V.12. No.2. P.129-134.
28. Shtykov S., Melnikov G., Goryacheva I. The effect of an external heavy atom on the sensitized room temperature phosphorescence in aqueous micellar solutions of sodium dodecylsulphate // J. Molec. Struct. 1999. V.482/483. P. 699-702.
27. Levshin L.V., Shtykov S.N., Goryacheva I.Yu., Melnikov G.V. Phosphorescence of polycyclic aromatic hydrocarbon molecules in aqueous micellar solutions of sodium dodecyl sulfate at room temperature // Zh. adj. spectrosk. 1999. T.66. No. 2. P.201-204.
26. Melnikov G.V., Goryacheva I.Yu., Shtykov S.N. Phosphorescence at room temperature sensitized by triplet-triplet energy transfer in micelles of sodium dodecyl sulfate // Dokl. Academician Sci. 1998. T.361. No. 1. P.72-73.
25. Melnikov G.V., Goryacheva I.Yu., Shtykov S.N. Luminescent analytical spectroscopy of polycyclic aromatic hydrocarbons based on triplet-triplet excitation energy transfer in micelles of anionic surfactants // Chimia. 1998. V. 52. No. 7/8. P. 416.
24. Shtykov S.N., Sumina E.G. Analytical capabilities of micellar mobile phases in TLC of 1,3-diketonates of some metals // Journal of analysis. chemistry. 1998. T.53, no. 5. pp. 508-513.
23. Shtykov S.N., Beloliptseva G.M. Effects of fluorescence enhancement and quenching in the magnesium-8-hydroxyquinoline-5-sulfonic acid cationic surfactant system and their analytical application // Journal. analyte chemistry. 1998.T.53, No. 3. P. 297-302.
22. Shtykov S.N., Goryacheva I.Yu. Analytical luminescence spectroscopy in microheterogeneous supra- and supramolecular self-associating organized media // Optics and Spectrosc. 1997. T.83, No. 4.S. 698-703.
21. Shtykov S.N., Klimov B.N., Smirnova T.D., Glukhovskoy E.G., Istrashkina E.V., Sumina E.G. Preparation and study of the properties of a Langmuir-Blodgett film based on methyl orange and polyamide acid // Journal. physical chemistry. 1997. T.71. No. 7. pp. 1292-1295.
20. Shtykov S.N., Sumina E.G., Malova M.I. Synergism and antagonism in nonionic surfactant electrolyte-micelle systems and their influence on the photometric and analytical characteristics of chromasurol S chelates // Zh. analyte chemistry. 1997. T.52, No. 7. P.707-712.
19. Shtykov S.N., Sumina E.G. Protolytic properties of chromasurol S in electrolyte solutions and micelles of nonionic surfactants // Journal. analyte chemistry. 1997. T.52, No. 7. P.697-702.
18. Shtykov S.N., Sumina E.G., Parshina E.V., Lopukhova S.S. Application of micellar mobile phases for the separation of fluorescein derivatives by TLC // Zhurn. analyte chemistry. 1995. T.50, No. 7. P.747-751.
17. Shtykov S.N., Parshina E.V. Microenvironment and properties of organic reagents in surfactant solutions // Journal. analyte chemistry. 1995. T.50. No. 7. P.740-746.
16. Shtykov S.N., Pankratov A.N., Lisenko N.F., Sumina E.G., Smirnova T.D. The relationship between fundamental and deductive principles of teaching analytical chemistry // Journal. analyte chemistry. 1995. T.50, No. 4. P.351-354.
15. Shtykov S.N., Parshina E.V., Bubelo V.D. Tautomeric equilibrium of b-diketones in micellar solutions of surfactants // Journal. analyte chemistry. 1994. T.49, No. 5. P.469-472.
14. Shtykov S.N., Parshina E.V. Keto-enol tautomerism in micellar solutions of surfactants // Journal. physical chemistry. 1994. T.68, No. 1. P.114-118.
13. Chernova R.K., Shtykov S.N. Hydrophobic ligand-ligand interactions in multicomponent systems and their analytical significance // Fresenius Ztschr. Anal. Chem. 1989. Bd.335, S.111-116
12. Shtykov S.N., Amelin V.G., Sorokin N.N., Chernova R.K. Deprotonation of cresol red in aqueous solution in the presence of cationic surfactants // Journal. physical chemistry. 1986. T.60, No. 2. P.345-349.
11. Tsepulin V.V., Kartsev V.N., Amelin V.G., Chernova R.K., Shtykov S.N. On the nature of hydration of the associate of sulfochrome with cetylpyridinium // Zhurn. physical chemistry. 1986. T.60, No. 1. P.232-234.
10. Chernova R.K., Kartsev V.N., Amelin V.G., Shtykov S.N. Hydration of cationic surfactants // Journal. physical chemistry. 1985. T.59, No. 11. P.2740-2743.
9. Shtykov S.N., Sumina E.G., Chernova R.K., Lemeshkina N.V. A new express method for the separate determination of nonionic and anionic surfactants in wastewater // Zhurn. analyte chemistry. 1985. T.40, No. 5. P.907-910.
8. Chernova R.K., Shtykov S.N., Beloliptseva G.M., Sukhova L.K., Amelin V.G., Kulapina E.G. Some questions of the mechanism of action of surfactants in systems of organic reagents - metal ions // Journal. analyte chemistry. 1984. T.39, No. 6. P.1019-1028.
7. Shtykov S.N., Sumina E.G., Chernova R.K., Semenenko E.V. The influence of strong electrolytes on the association of organic analytical reagents with cationic surfactants // Zhurn. analyte chemistry. 1984. T.39, no. 6. P.1029-1033
6. Chernova R.K., Amelin V.G., Shtykov S.N. The influence of cationic surfactants on the nature of hydration and some properties of triphenylmethane compounds in aqueous solutions // Zhurn. physical chemistry. 1983. T.57, No. 6. P.1482-1485.
5. Smirnova T.D., Chernova R.K., Shtykov S.N. Synthesis and study of the physicochemical properties of a germanium (IV) complex with pyrocatechol violet and cetylpyridinium chloride // Journal. inorganic chemistry. 1983. T.28, No. 11. P.2814-2817.
4. Savvin S.B., Marov I.N., Chernova R.K., Shtykov S.N., Sokolov A.B. Electrostatic and hydrophobic effects in the formation of associates of organic reagents with cationic surfactants // Zhurn. analyte chemistry. 1981. T.36, No. 5. P.850-859.
3. Savvin S.B., Marov I.N., Chernova R.K., Kudryavtseva L.M., Shtykov S.N., Sokolov A.B. On the interaction of nonionic surfactants with phenolcarboxylic acids of the triphenylmethane series // Zhurn. analyte chemistry. 1981. T.36, No. 8. P.1461-1470.
2. Savvin S.B., Chernova R.K., Belousova V.V., Sukhova L.K., Shtykov S.N. On the mechanism of action of cationic surfactants in organic reagent-metal ion-surfactant systems // Journal. analyte chemistry. 1978. T.33, No. 8. P.1473-1484.
1. Savvin S.B., Chernova R.K., Shtykov S.N. Associates of some azo compounds with long-chain quaternary ammonium salts and their use in the analysis of organic reagents // Journal. analyte chemistry. 1978. T.33. No. 5. P.865-870.
Victories in grants and scientific projects:
- RFBR grant, No. 94-03-08759a, 1994-1996. “Organized systems in analysis” - leader 2. Grant of the Russian Foundation for Basic Research, No. 97-03-33393a, 1997-1999. “Microheterogeneous organized environments based on supra- and supramolecular systems in analytical chemistry” - leader 3. RFBR grant No. 98-03-42876з for a trip to a foreign conference (European Congress on Molecular Spectroscopy - EUCMOS XXIV, Prague, 1998) 4. RFBR grant No. 99-03-42724з for a trip to the IUPAC General Assembly, August 1999. 5. Grant for holding the All-Russian conference with international participation “Organic reagents in analytical chemistry” No. 99-03-42018g, September 1999 6. Grant RFBR, No. 01-03-32649a, 2001-2003. “Self-organizing supramolecular systems in analytical chemistry” - leader 7. RFBR grant No. 04-03-32496a, 2004-2006. “Development of a strategy for the use of nanoreactors based on organized media in chemical analysis” - head 8. RFBR grant 05-03-33178a 2005-2007. “Theoretical and experimental study of a new version of thin-layer chromatography with a time-varying gas phase” - performer 9. State contract of the Agency for Science and Innovation of the Ministry of Education and Science No. 02.513.11.3028, 2007 “Creation of membranes and catalytic systems based on nanotechnology, nanosystems and self-assembly principles” - head 10. RFBR grant No. 08-03-00725a, 2008-2010. “Nanosystems and principles of supramolecular chemistry in chemical analysis” - head 11. RFBR Grant No. 09-03-00245a, 2009-2011 “Functionalization of the surface of the dispersed phase of emulsion systems with inorganic nanoparticles” - executor 12. RFBR Grant No. 07-03-06052 “Organization and holding the Analytical Russian-German-Ukrainian Symposium (ARGUS) Nanoanalytics”, August 25-28. 2007 – head 13. RFBR Grant No. 09-03-11502с, 2009 for the best popular science article “Organized media - the world of liquid nanosystems” – head 14. RFBR Grant No. 07-03-08343з “Participation in the EUROANALYSIS conference XIV, organized by the European Association of Chemical and Molecular Sciences (EuCheMS), and participation in the work of the EuCheMS Department of Analytical Chemistry", Antwerp, Belgium, September 2007. 15. RFBR Grant No. 09-03-08229з "Participation in the EUROANALYSIS 2009 conference under the auspices European Association of Chemical and Molecular Sciences (EuCheMS) and the work of the Department of Analytical Chemistry (DAC EuCheMS) as a representative of the Russian Chemical Society. D.I.Mendeleev" 2009, Innsbruck, Austria, September 6-10. 2009 16. State contract 02. 740.11.0879 “Development of new photonic technologies for analyzing biophysical processes in living organisms at the subcellular, cellular and tissue levels for the tasks of non-invasive and minimally invasive diagnostics and therapy.” 2010-2012 - executor 17. RFBR No. 12-03-00450a, “Nanoobjects and nanotechnologies in chemical analysis”, 2012-2014. – head of 18. RFBR 13-03-00360a “Development of analytical methodology for deciphering human metal scrap.” 2013-2015 – performer 19. RFBR No. 15-03-99704a, “Synthesis, modification and application of magnetic nanoparticles for the concentration and determination of biologically active substances”, 2015-2017. – head 20. RFBR grant 15-03-07015d “Nanoobjects and nanotechnologies in chemical analysis” - publication of a monograph. 2015 - head 21. RFBR grant 18-03-01029a “Separation, concentration and determination of biologically active substances using solid and liquid nanoobjects as tools for chemical analysis” 2018-2020. - supervisor. 22. Project part of the state task of the Ministry of Education and Science No. 4.1212.2014/K "Creation of chemical substances and materials for new systems with sensory, catalytic, extraction and energy-generating properties", 2014-2016 - head 23. RSF 14-12-00275 "Research of charge transfer and absorption and photoluminescence spectra in ordered systems “nanoparticles in an organic matrix” and the development of physical and technological foundations for creating the elemental base of molecular electronics”; 2014-2016 – executor 24. RFBR grant 16-03-00492a “Development of analytical methodology for the development of medical products based on metal-containing nanomaterials.” 2016-2018 - performer 25. Grant of the Ministry of General and Professional Education (1996-1997), "Fundamental research in the field of agricultural machinery" section - "Machines for the food industry" (Center - Rostov-on-Don, Krasnodar) - head 26. Grant from the Ministry of General and Vocational Education, No. 97-0-9.5-40, 1998-2000. “Research in the field of fundamental natural science.” (Center - St. Petersburg) - head 27. Grant of the Ministry of Higher Education No. E00–5.0–253, 2000-2001. (Center - St. Petersburg) - head 28. Grant of the Ministry of Higher Education No. E02–5.0–65, 2002-2003. (Center - St. Petersburg) - head
Additional Information:
During the work, more than 650 oral and poster presentations were made at foreign, international, all-Russian and some regional conferences, more than 650 abstracts of reports were published. More than 70 reports are plenary, keynote, invited and sectional oral in English and Russian, made in Japan, France, Germany, Poland, Denmark, Sweden, Spain, Serbia, Czech Republic, Russia.
Expertise
1. Expert of the Federal Target Program competition of the Ministry of Education and Science of the Russian Federation for receiving grants from the Government of the Russian Federation for state support of scientific research conducted under the guidance of leading scientists in Russian educational institutions of higher professional education (Resolution of the Government of the Russian Federation dated 04.2010 No. 220)
2. Expert of the Russian Foundation for Basic Research
Nanochemistry and nanotechnology, IDPO SSU (Saratov), 2017
Preface to the series “Analytical reagents.................................................................. .... 5
List of main abbreviations................................................................... .......................... 9
Introduction........................................................ .............................. 12
Chapter 1. Main types of surfactants used
in analysis. Mugods of their synthesis and properties.................................................... 17
Types of surfactants................................................................. ..... 17
Synthesis of surfactants................................................................. ... 22
Purification and determination of the main substance in surfactants.................................................. ......... 29
Specific behavior of surfactants in aqueous solutions.................................................. ........................... 33
Chapter d. Modification of organic reagents with surfactants.................................................. ........................................ 48
Ionic association of organic reagents with surfactants
substances........................................................ ..................................... 48
The influence of the concentration of surfactants and strong electrolytes on the ionic association.................................................... .................... 70
Specificity of associates of chromophore organic reagents with hachi
onic surfactants.................................................................... 75
Modification of the properties of organic analytical reagents during their solubilization in micelles of anionic and nonionic surfactants................................................... .................................. 76
Chapter 3. Chemical-analytical properties of modified reagents.................................................. ........................ 80
Hydration of modified reagents.................................................... 80
The influence of surfactants on protollonic equilibria
in reagent solutions............................................................. ........................... 84
Complex-forming properties of associates.................................................... 89
Effect of strong electrolytes on complex formation in M systems
K---surfactant................................................... ........................................ 103
Influence of the fourth component on the M---R---surfactant systems.................................... 107
The influence of surfactants on the rate of reactions.................................. 117
Chapter 4. Application of modified reagents in photometric
analysis........................................................ .................................... 120
Elements of group I................................................... ........................... 121
Elements of group II................................................... ........................... 124
Elements of group III................................................... ............................... 130
Elements of group IV................................................... ............................ 142
Elements of group V................................................... ........................... 151
Elements of group VI................................................... ........................ 155
Elements of group VII................................................... ............................... 161
Elements of the GS group................................................... ........................... 161
Chapter 5. Use of surfactants in other methods
analysis........................................................ ........................................... 170
Titrimetric analysis................................................... ................... 170
Luminescent analysis................................................... .................... 173
Atomic absorption and atomic emission methods of analysis.................................. 183
Electrochemical methods of analysis................................................................... ...... 186
Methods of separation and concentration.................................................................... 189
Literature................................................. .................................. 205
